A Facile Reaction of Unactivated Imines with Telluronium Allylide. Highly Stereoselective Synthesis of Vinylaziridines

نویسندگان

  • Wei-Wei Liao
  • Xian-Ming Deng
  • Yong Tang
  • Fenglin Lu
چکیده

Supporting Information General methods. Infrared spectra were recorded on a Nicolet AVATAR-360 spectrometer. H NMR and C NMR spectra were recorded at Bruker AM-300 instruments. Low resolution mass spectra (m/z) were recorded on HP5989A. High-resolution mass spectra were recorded on Concept 1H or MALDI/DHB. Microanalyses were performed using a Elemantar Vario EL. All reaction flasks were dried by flame. And all reactions were carried out under argon unless otherwise noted. THF and toluene were dried by distilled over sodium-benzophenone ketyl prior to use. N-aryl imines and -amidoalkyl-p-tolyl sulfones were prepared according to literature methods.

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تاریخ انتشار 2004